氧氮氢分析仪的常见故障及解决方法：氧和氮空白值超过20。这是由于气流小，不能将炉子中的空气驱赶出去。可调节气体流量，调节载气压力在0.2~0.4MPa。接通仪器载气，放一个石墨坩埚在下电极上，打开主电源开关，点击软件上的关炉按钮，关闭炉子并等待10s。调节流量调节器，直到流量计a显示为30L／h，打开炉子。调节调节器直到流量计b显示为50L／h，再次关闭炉子。如果以上设置不稳定，则增加流量至100L／h，反复调节直至仪器稳定。上海禹重实业有限公司分析仪获得众多用户的认可。江苏进口分析仪多少钱

Procedure-SolidSamplesDeterminetheinstrumentblank.Repeatsteps2bthrough2gaminimumofthreetimes.Settheblankfollowingtheprocedureoutlinedintheoperatorsinstructionmanual.Instrumentcalibration/driftcorrection.Loginaminimumof3Standardreplicates.Weighapproximately***gramsofacalibration/driftstandard,enterthemassandstandardidentificationintoappropriatereplicatefields.Note:LECOReferenceMateria***onotrequirepreparation.Seepreparationstatementonthereferencematerialcertificate.山东美国分析仪哪家好上海禹重实业有限公司致力于提供分析仪，竭诚为您服务。

SamplePreparationSamplingandsamplepreparationofrefractorymetalssuchastitaniumandzirconiumissomewhatdifferentfromthatofsteel.Unlikesteelsamples,hydrogenisnotasmobileinthisgroupofmaterials;therefore,storageinliquidnitrogenordryiceisnotrequired.However,itisimportanttokeepthesamplecoolwhencuttingorsectioning.Samplepreparationforoxygenandnitrogendeterminationhasbeendifferentfromthatofhydrogendetermination.

SamplePreparationSamplingandsamplepreparationisanimportantissuebecausetraditionalmethodsusedtoobtainsamplesforoxygenandnitrogendeterminationaredifferentfromthoserecommendedforhydrogen,especiallywhensamplingmoltenmetal.Themaindifferenceinsteelsamplingproceduresforoxygen/nitrogenandhydrogenisduetothemobilityofhydrogen.Specialprecautionsmustbeusedwhensamplingforhydrogen.Frommoltensteelandiron,asamplemustbequicklyquenchedincoldwaterandchilledinarefrigerantsuchasliquefiednitrogenoramixtureofacetoneandsolidcarbondioxideinordertoreducelossesofhydrogenfromdiffusion.Lossesofoxygenandnitrogenfromdiffusionarenotaproblem.Asamplethatistakenforhydrogenandchilledinarefrigerantcanalsobeusedforoxygenandnitrogendetermination.However,asamplethatistypicallytakenforoxygenand/ornitrogendeterminationisnotsuitableforhydrogendeterminationduetohydrogenloss(diffusion).Surfacecontaminationmustberemovedbyfilingorlightgrinding,usingcarenottooverheatthesample.上海禹重实业有限公司为您提供分析仪，期待您的光临！

Procedure-SolidSamples：--Instrumentcalibration/driftcorrection.Placethenickelbasketcontainingthecalibration/driftstandardintotheopenportatthetopoftheloadinghead.PresstheAnalyzebuttonontheinstrumentscreenagain,theloadingheadslide-blockwillcloseandthelowerelectrodewillopen.Cleantheupperandlowerelectrodemanually,or,ifapplicable,removethecrucibleandpresstheanalyzebuttontocleanwiththeautomaticcleaner.分析仪，就选上海禹重实业有限公司，让您满意，欢迎您的来电哦！北京元素分析仪供应商

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氧氮氢分析仪的优点采用惰气熔融技术，同时测定氧、氮和氢元素含量新设计封闭气路系统，优化气路循环，使氧氮氢测量更准确可采用更廉价的氩气作为载气催化炉温度可调，使氧的测量更加准确气路系统都采用电磁阀控制，新增分段式漏气检测水冷样品加样端口，有效隔绝杂质气体侵入仪器配置和氧、氮、氢测量范围可灵活选择新设计的高灵敏度红外检测池和热导池，有极低的检出限分析时间短脉冲炉功率高达8.5kw，温度3000℃颗粒状样品无需胶囊包裹，使用经济实惠化学试剂及管路隐藏在门后（可移除）强大的分析软件（支持数据和应用报告导出、增加评论区及其他更多功能）。单点和多点校正（线性回归）可采用自来水、冷却循环水机或交换机冷却新设计的产品可用于各类生产控制和实验室。江苏进口分析仪多少钱